4LL9
Crystal structure of D3D4 domain of the LILRB1 molecule
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL17U |
| Synchrotron site | SSRF |
| Beamline | BL17U |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2012-10-12 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 1.0000 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 121.257, 71.976, 75.036 |
| Unit cell angles | 90.00, 95.20, 90.00 |
Refinement procedure
| Resolution | 32.808 - 2.686 |
| R-factor | 0.2464 |
| Rwork | 0.245 |
| R-free | 0.27480 |
| Structure solution method | SAD |
| RMSD bond length | 0.005 |
| RMSD bond angle | 1.239 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | SHELXS |
| Refinement software | PHENIX ((phenix.refine: 1.8.2_1309)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.800 |
| High resolution limit [Å] | 2.686 | 2.700 |
| Number of reflections | 17596 | |
| Completeness [%] | 97.5 | 96.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6.9 | 277 | 0.2M NaI, pH 6.9, VAPOR DIFFUSION, SITTING DROP, temperature 277K |
