4LDK
FAD-linked sulfhydryl oxidase ALR mutation
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RUH3R |
| Temperature [K] | 93 |
| Detector technology | IMAGE PLATE |
| Collection date | 2012-03-19 |
| Detector | RIGAKU RAXIS IV |
| Wavelength(s) | 1.54178 |
| Spacegroup name | C 2 2 21 |
| Unit cell lengths | 50.897, 77.770, 62.772 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 23.580 - 2.040 |
| R-factor | 0.19848 |
| Rwork | 0.195 |
| R-free | 0.26664 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3mbg |
| RMSD bond length | 0.020 |
| RMSD bond angle | 1.981 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | CCP4 |
| Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 2.040 |
| Number of reflections | 15237 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 6.5 | 298 | VAPOR DIFFUSION, Hanging drop, pH 6.5, temperature 298K |
