4L43
Crystal structures of human p70S6K1-T389A (form I)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-03-28 |
Detector | CCD ADSC unsupported-q315 |
Wavelength(s) | 0.9797 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 79.572, 79.572, 112.749 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 50.000 - 3.000 |
R-factor | 0.22929 |
Rwork | 0.227 |
R-free | 0.27890 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.028 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 3.110 |
High resolution limit [Å] | 3.000 | 6.460 | 3.000 |
Rmerge | 0.098 | 0.049 | 0.520 |
Number of reflections | 8690 | ||
<I/σ(I)> | 8.4 | ||
Completeness [%] | 99.9 | 99.4 | 100 |
Redundancy | 6.9 | 6.4 | 7.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 289 | 1.6M ammonium citrate, 0.1M Bis-Tris propane, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 289K |