4KZI
Crystal Structure of TR3 LBD in complex with DPDO
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-04-27 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.98 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 74.723, 76.512, 128.918 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.280 - 2.410 |
R-factor | 0.2083 |
Rwork | 0.206 |
R-free | 0.24860 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.016 |
RMSD bond angle | 1.787 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.440 |
High resolution limit [Å] | 2.400 | 6.510 | 2.400 |
Rmerge | 0.085 | 0.059 | 0.455 |
Number of reflections | 29201 | ||
<I/σ(I)> | 9 | ||
Completeness [%] | 99.4 | 90.6 | 100 |
Redundancy | 4.7 | 3.8 | 4.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 4.2 | 277 | PEG 4000, Sodium citrate, Glycerol, pH 4.2, vapor diffusion, temperature 277K |