4KNT
Copper nitrite reductase from Nitrosomonas europaea pH 8.5
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 21-ID-D |
| Synchrotron site | APS |
| Beamline | 21-ID-D |
| Detector technology | CCD |
| Collection date | 2011-07-11 |
| Detector | MARMOSAIC 300 mm CCD |
| Wavelength(s) | 1.3776 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 99.868, 123.090, 88.431 |
| Unit cell angles | 90.00, 97.23, 90.00 |
Refinement procedure
| Resolution | 34.110 - 1.900 |
| R-factor | 0.17102 |
| Rwork | 0.170 |
| R-free | 0.19997 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.027 |
| Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 34.110 |
| High resolution limit [Å] | 1.900 |
| Number of reflections | 78099 |
| Completeness [%] | 98.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
