4KDR

Crystal Structure of UBIG/SAH complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU RUH3R
Temperature [K]	100
Detector technology	IMAGE PLATE
Detector	MAR scanner 345 mm plate
Wavelength(s)	0.9793
Spacegroup name	C 1 2 1
Unit cell lengths	141.133, 39.500, 40.422
Unit cell angles	90.00, 94.40, 90.00

Refinement procedure

Resolution	38.030 - 2.003
R-factor	0.1913
Rwork	0.189
R-free	0.23300
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	1.096
Data reduction software	HKL-2000
Data scaling software	SCALA
Phasing software	MOLREP
Refinement software	PHENIX (1.8.2_1309)

Data quality characteristics

	Overall
Low resolution limit [Å]	38.030
High resolution limit [Å]	2.003

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	5	287	0.1M citric acid PH 5.0 and 20% v/v 2-Methyl-2,4-pentanediol, VAPOR DIFFUSION, HANGING DROP, temperature 287K