4KDC
Crystal Structure of UBIG
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RUH3R |
| Temperature [K] | 287 |
| Detector technology | IMAGE PLATE |
| Collection date | 2010-06-12 |
| Detector | MAR scanner 345 mm plate |
| Wavelength(s) | 0.9994 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 119.848, 58.584, 40.168 |
| Unit cell angles | 90.00, 105.26, 90.00 |
Refinement procedure
| Resolution | 29.510 - 2.090 |
| R-factor | 0.18482 |
| Rwork | 0.183 |
| R-free | 0.22459 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.232 |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALA |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 29.510 |
| High resolution limit [Å] | 2.090 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 287 | 0.1M HEPES pH7.5 and 20% polyethylene glycol 10000, VAPOR DIFFUSION, HANGING DROP, temperature 287K |
