4JNB
Crystal structure of the Catalytic Domain of Human DUSP12
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PAL/PLS BEAMLINE 4A |
| Synchrotron site | PAL/PLS |
| Beamline | 4A |
| Spacegroup name | H 3 |
| Unit cell lengths | 127.380, 127.380, 40.280 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 50.000 - 3.000 |
| Rwork | 0.247 |
| R-free | 0.25300 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Refinement software | CNS |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 3.000 |
| Number of reflections | 4743 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 8.5 | 298 | 0.1M Tris pH 8.5, 1.9M Ammonium sulfate, VAPOR DIFFUSION, temperature 298K |
