4JAB
U/G Wobble Base Pair in a RNA Duplex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.2 |
Synchrotron site | ALS |
Beamline | 8.2.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-12-14 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97895 |
Spacegroup name | H 3 |
Unit cell lengths | 41.681, 41.681, 60.014 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 30.930 - 2.230 |
R-factor | 0.15648 |
Rwork | 0.152 |
R-free | 0.22898 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 246d |
RMSD bond length | 0.009 |
RMSD bond angle | 2.093 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.930 | 2.310 |
High resolution limit [Å] | 2.230 | 2.230 |
Rmerge | 0.066 | 0.330 |
Number of reflections | 1723 | |
Completeness [%] | 91.0 | 90.1 |
Redundancy | 2.2 | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | VAPOR DIFFUSION, HANGING DROP |