4J7W
E3_5 DARPin L86A mutant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2011-02-23 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 44.370, 78.590, 82.230 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.115 - 1.600 |
R-factor | 0.1627 |
Rwork | 0.162 |
R-free | 0.18620 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.021 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.8_1069)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.640 |
High resolution limit [Å] | 1.600 | 1.600 |
Number of reflections | 38289 | |
Completeness [%] | 98.9 | 99.4 |
Redundancy | 8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.6 | 293.15 | 0.1 M Na-Citrate, 20% 2-propanol, 20% PEG4000, pH 5.6, VAPOR DIFFUSION, SITTING DROP, temperature 293.15K |