4J4V

Pentameric SFTSVN with suramin

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PHOTON FACTORY BEAMLINE BL-17A
Synchrotron site	Photon Factory
Beamline	BL-17A
Temperature [K]	100
Detector technology	CCD
Collection date	2012-05-15
Detector	ADSC QUANTUM 315
Wavelength(s)	0.97
Spacegroup name	C 1 2 1
Unit cell lengths	103.145, 154.888, 93.291
Unit cell angles	90.00, 102.12, 90.00

Refinement procedure

Resolution	42.717 - 2.303
R-factor	0.2245
Rwork	0.223
R-free	0.26060
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	4j4r
RMSD bond length	0.007
RMSD bond angle	1.052
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASES
Refinement software	PHENIX ((phenix.refine: 1.8.1_1168))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	42.720	2.380
High resolution limit [Å]	2.300	2.300
Number of reflections	60718
Completeness [%]	96.1	79.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1