Loading
PDBj
MenuPDBj@FacebookPDBj@X(formerly Twitter)PDBj@BlueSkyPDBj@YouTubewwPDB FoundationwwPDBDonate
RCSB PDBPDBeBMRBAdv. SearchSearch help

4IVN

The Vibrio vulnificus NanR protein complexed with ManNAc-6P

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsPHOTON FACTORY BEAMLINE BL-17A
Synchrotron sitePhoton Factory
BeamlineBL-17A
Temperature [K]100.15
Detector technologyCCD
Collection date2012-06-08
Wavelength(s)1.0000
Spacegroup nameP 31 2 1
Unit cell lengths109.205, 109.205, 82.472
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution30.000 - 1.900
R-factor0.18321
Rwork0.181
R-free0.23487
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.021
RMSD bond angle2.126
Refinement softwareREFMAC (5.6.0117)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0001.930
High resolution limit [Å]1.9001.900
Number of reflections45033
Completeness [%]99.9100
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP5294.1510% PEG 2000 MME, 0.1M ammonium sulfate, 0.3M sodium formate, 3% PGA-LM, 0.1M sodium acetate, pH 5.0, VAPOR DIFFUSION, SITTING DROP, temperature 294.15K

229380

PDB entries from 2024-12-25

PDB statisticsPDBj update infoContact PDBjnumon