4IAS
HEW Lysozyme by langmuir- blodgett modified vapour diffusion
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Wavelength(s) | 0.932 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 78.730, 78.730, 37.010 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 55.670 - 2.600 |
R-factor | 0.2095 |
Rwork | 0.205 |
R-free | 0.30110 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.013 |
RMSD bond angle | 1.385 |
Data reduction software | MOSFLM |
Data scaling software | SCALA (3.3.16) |
Phasing software | MOLREP |
Refinement software | REFMAC |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 55.671 | 39.365 | 2.740 |
High resolution limit [Å] | 2.600 | 8.220 | 2.600 |
Rmerge | 0.059 | 0.640 | |
Total number of observations | 1622 | 7170 | |
Number of reflections | 3906 | ||
<I/σ(I)> | 20.1 | 10.1 | 0.9 |
Completeness [%] | 100.0 | 99.5 | 100 |
Redundancy | 12.3 | 10.1 | 13.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |