4I7V
Agrobacterium tumefaciens DHDPS with pyruvate
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX1 |
| Synchrotron site | Australian Synchrotron |
| Beamline | MX1 |
| Wavelength(s) | 0.9536 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 182.770, 77.030, 98.940 |
| Unit cell angles | 90.00, 121.16, 90.00 |
Refinement procedure
| Resolution | 84.670 - 1.450 |
| R-factor | 0.1614 |
| Rwork | 0.160 |
| R-free | 0.17976 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.215 |
| Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 84.670 |
| High resolution limit [Å] | 1.430 |
| Number of reflections | 207498 |
| Completeness [%] | 96.0 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 293 | 0.1 M Tris pH 8.5, 2 M ammonium sulphate, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
