4HOQ

Crystal Structure of Full-Length Human IFIT5

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	CLSI BEAMLINE 08ID-1
Synchrotron site	CLSI
Beamline	08ID-1
Temperature [K]	105
Detector technology	CCD
Collection date	2011-01-01
Detector	MARMOSAIC 300 mm CCD
Wavelength(s)	0.979
Spacegroup name	P 21 21 21
Unit cell lengths	64.150, 71.428, 117.560
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	37.051 - 2.070
R-factor	0.1683
Rwork	0.165
R-free	0.21280
Structure solution method	SAD
RMSD bond length	0.006
RMSD bond angle	0.944
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	SHELXS
Refinement software	PHENIX ((phenix.refine: 1.8.1_1168))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.140
High resolution limit [Å]	2.000	2.070
Number of reflections	37620
Completeness [%]	96.1	78.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7.5	277.15	pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 277.15K