4HED

Zebrafish chemokine CXL1

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	NSLS BEAMLINE X25
Synchrotron site	NSLS
Beamline	X25
Wavelength(s)	1.0
Spacegroup name	P 21 21 2
Unit cell lengths	46.330, 56.770, 27.670
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	28.385 - 1.620
R-factor	0.1819
Rwork	0.180
R-free	0.23010
Structure solution method	SAD
RMSD bond length	0.009
RMSD bond angle	1.327
Refinement software	PHENIX ((phenix.refine: 1.8_1069))

Data quality characteristics

	Overall
Low resolution limit [Å]	46.310
High resolution limit [Å]	1.620
Number of reflections	9709

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7.4	298	0.1M Tris, 38% PEG 3350, pH 7.4, VAPOR DIFFUSION, HANGING DROP, temperature 298K