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4H8G

crystal structure of a parallel 6-helix coiled coil CC-Hex-IL- 22

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I04
Synchrotron siteDiamond
BeamlineI04
Detector technologyCCD
DetectorADSC QUANTUM 315
Wavelength(s)0.97
Spacegroup nameC 2 2 21
Unit cell lengths51.990, 126.800, 127.530
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution38.400 - 1.699
R-factor0.24873
Rwork0.247
R-free0.27974
Structure solution methodSAD
RMSD bond length0.009
RMSD bond angle1.152
Refinement softwareREFMAC (5.6.0117)
Data quality characteristics
 Overall
Low resolution limit [Å]69.200
High resolution limit [Å]1.699
Number of reflections46623
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1
1

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