4H8G
crystal structure of a parallel 6-helix coiled coil CC-Hex-IL- 22
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Detector technology | CCD |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 51.990, 126.800, 127.530 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.400 - 1.699 |
R-factor | 0.24873 |
Rwork | 0.247 |
R-free | 0.27974 |
Structure solution method | SAD |
RMSD bond length | 0.009 |
RMSD bond angle | 1.152 |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 69.200 |
High resolution limit [Å] | 1.699 |
Number of reflections | 46623 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | ||||
1 |