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4H4R

Crystal Structure of Ferredoxin reductase, BphA4 E175C/Q177G mutant (oxidized form)

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsPHOTON FACTORY BEAMLINE AR-NE3A
Synchrotron sitePhoton Factory
BeamlineAR-NE3A
Temperature [K]95
Detector technologyCCD
Collection date2010-11-19
DetectorADSC QUANTUM 270
Wavelength(s)0.98008
Spacegroup nameP 61 2 2
Unit cell lengths98.456, 98.456, 170.721
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution60.325 - 1.400
R-factor0.1985
Rwork0.198
R-free0.21590
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2gqw
RMSD bond length0.006
RMSD bond angle1.169
Data reduction softwareXDS
Data scaling softwareXSCALE
Phasing softwareMOLREP
Refinement softwarePHENIX ((phenix.refine: 1.8_1069))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]60.3301.480
High resolution limit [Å]1.4001.400
Number of reflections95862
Completeness [%]99.5100
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP5.42932.5M Sodium formate, 0.1M acetate buffer, pH 5.4, VAPOR DIFFUSION, SITTING DROP, temperature 293K

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