4GX5
GsuK Channel
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-D |
Synchrotron site | APS |
Beamline | 23-ID-D |
Temperature [K] | 78 |
Detector technology | CCD |
Collection date | 2010-03-04 |
Detector | MARMOSAIC 300 mm CCD |
Wavelength(s) | 1.03319 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 234.976, 108.364, 165.787 |
Unit cell angles | 90.00, 134.96, 90.00 |
Refinement procedure
Resolution | 45.393 - 3.700 |
R-factor | 0.2623 |
Rwork | 0.261 |
R-free | 0.29290 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.053 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.7.3_928)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.760 |
High resolution limit [Å] | 3.700 | 3.700 |
Number of reflections | 27539 | |
Completeness [%] | 86.7 | 47.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 9 | 293 | 13-18% PEG 3350, 250-500mM KSCN, 100mM CHES, pH 9.0, VAPOR DIFFUSION, SITTING DROP, temperature 293K |