4GQZ
Crystal Structure of S.CueP
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL44B2 |
| Synchrotron site | SPring-8 |
| Beamline | BL44B2 |
| Temperature [K] | 77 |
| Detector technology | CCD |
| Collection date | 2011-06-30 |
| Detector | ADSC QUANTUM 210 |
| Wavelength(s) | 0.9790, 0.9792, 0.9900 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 58.456, 102.160, 114.238 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 40.854 - 1.799 |
| R-factor | 0.2294 |
| Rwork | 0.228 |
| R-free | 0.27580 |
| Structure solution method | MAD |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.120 |
| Data reduction software | DENZO |
| Data scaling software | HKL-2000 |
| Phasing software | SOLVE |
| Refinement software | PHENIX ((phenix.refine: 1.8_1069)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.830 |
| High resolution limit [Å] | 1.799 | 1.800 |
| Number of reflections | 118693 | |
| Completeness [%] | 19.7 | 81.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 287 | 0.1M sodium acetate, 2.0M sodium chloride , pH 4.6, VAPOR DIFFUSION, HANGING DROP, temperature 287K |
