4GFL
NO mechanism, slma
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALS BEAMLINE 8.3.1 |
| Synchrotron site | ALS |
| Beamline | 8.3.1 |
| Detector technology | CCD |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 1.111 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 71.920, 40.860, 76.430 |
| Unit cell angles | 90.00, 111.80, 90.00 |
Refinement procedure
| Resolution | 70.970 - 2.300 |
| R-factor | 0.238 |
| Rwork | 0.238 |
| R-free | 0.27800 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.022 |
| RMSD bond angle | 1.600 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | MOLREP |
| Refinement software | CNS (1.2) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 71.000 |
| High resolution limit [Å] | 2.300 |
| Number of reflections | 20000 |
| Completeness [%] | 95.0 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8 | 298 | tartrate, pH 8, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
