4GEU
Structure of a stabilised ceSAS-6 dimer
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I24 |
| Synchrotron site | Diamond |
| Beamline | I24 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2012-02-03 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.9687 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 70.580, 74.040, 81.070 |
| Unit cell angles | 90.00, 98.43, 90.00 |
Refinement procedure
| Resolution | 80.190 - 2.650 |
| R-factor | 0.2016 |
| Rwork | 0.200 |
| R-free | 0.22860 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.170 |
| Data reduction software | xia2 |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | BUSTER (2.10.0) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 80.190 | 2.790 |
| High resolution limit [Å] | 2.650 | 2.650 |
| Number of reflections | 24219 | |
| Completeness [%] | 99.0 | 99.8 |
| Redundancy | 3.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7 | 277 | 0.2M Calcium acetate hydrate, 20% (w/v) PEG 3350, pH 7, VAPOR DIFFUSION, SITTING DROP, temperature 277K |
