4GEN
Crystal structure of Zucchini (monomer)
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL32XU |
Synchrotron site | SPring-8 |
Beamline | BL32XU |
Collection date | 2011-12-07 |
Wavelength(s) | 0.9793, 0.9800 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 35.277, 52.396, 38.791 |
Unit cell angles | 90.00, 104.94, 90.00 |
Refinement procedure
Resolution | 37.480 - 2.200 |
R-factor | 0.225 |
Rwork | 0.223 |
R-free | 0.26990 |
Structure solution method | MAD |
RMSD bond length | 0.002 |
RMSD bond angle | 0.566 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | PHENIX (1.7.2_869) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.240 |
High resolution limit [Å] | 2.200 | 5.970 | 2.200 |
Rmerge | 0.097 | 0.061 | 0.354 |
Number of reflections | 6839 | ||
<I/σ(I)> | 10.8 | ||
Completeness [%] | 97.1 | 98.4 | 94.6 |
Redundancy | 5.4 | 6.9 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | vapor diffusion |