4GEJ
N-terminal domain of VDUP-1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX1 |
Synchrotron site | Australian Synchrotron |
Beamline | MX1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-10-11 |
Detector | ADSC QUANTUM 210r |
Wavelength(s) | 0.9537 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 79.740, 178.810, 81.890 |
Unit cell angles | 90.00, 113.32, 90.00 |
Refinement procedure
Resolution | 46.000 - 2.900 |
R-factor | 0.224 |
Rwork | 0.212 |
R-free | 0.29360 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.013 |
RMSD bond angle | 1.817 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.710 | 3.060 |
High resolution limit [Å] | 2.900 | 2.900 |
Rmerge | 0.075 | 0.665 |
Number of reflections | 46358 | |
<I/σ(I)> | 18.5 | 2.9 |
Completeness [%] | 99.5 | 98.8 |
Redundancy | 7.2 | 6.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 295 | 0.1 M Hepes, 0.2 M Calcium Acetate, 10-12% PEG monomethyl ether 5000, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 295K |