4G9M
Crystal structure of the Rhizoctonia solani agglutinin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX II BEAMLINE I911-2 |
Synchrotron site | MAX II |
Beamline | I911-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-10-20 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 1.03954 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 121.979, 61.091, 32.793 |
Unit cell angles | 90.00, 93.00, 90.00 |
Refinement procedure
Resolution | 20.734 - 1.601 |
R-factor | 0.184 |
Rwork | 0.181 |
R-free | 0.23200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2x2s |
RMSD bond length | 0.006 |
RMSD bond angle | 1.097 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MrBUMP |
Refinement software | PHENIX ((phenix.refine: 1.7.3_928)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.734 | 1.660 |
High resolution limit [Å] | 1.600 | 1.600 |
Number of reflections | 27436 | |
<I/σ(I)> | 4.9 | 1.5 |
Completeness [%] | 86.4 | 37.5 |
Redundancy | 14.63 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.2 | 289 | 0.1 M sodium acetate, pH 4.2, 20% v/v PEG8000, 0.2 M sodium chloride, 10 mM sodium citrate, VAPOR DIFFUSION, SITTING DROP, temperature 289K |