4G42
Structure of the Chicken MHC Class I Molecule BF2*0401 complexed to pepitde P8D
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 298 |
Detector technology | IMAGE PLATE |
Collection date | 2009-06-03 |
Detector | RIGAKU RAXIS VII |
Wavelength(s) | 1.5418 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 165.832, 40.108, 130.952 |
Unit cell angles | 90.00, 119.56, 90.00 |
Refinement procedure
Resolution | 40.627 - 2.294 |
R-factor | 0.199 |
Rwork | 0.196 |
R-free | 0.25400 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.005 |
RMSD bond angle | 0.942 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.627 | 2.400 |
High resolution limit [Å] | 2.294 | 2.300 |
Rmerge | 0.196 | |
Number of reflections | 33771 | |
<I/σ(I)> | 7.5 | |
Completeness [%] | 75.0 | 75 |
Redundancy | 4.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 291 | 5% MPD, 20% PEG 6000, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 291K |