4G2L
Human PDE9 in complex with selective compound
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Detector technology | CCD |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 104.226, 104.226, 270.476 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.810 - 3.000 |
R-factor | 0.18585 |
Rwork | 0.182 |
R-free | 0.21439 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.021 |
RMSD bond angle | 1.869 |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 3.000 |
Number of reflections | 30608 |
Completeness [%] | 99.0 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |