4FZQ

Crystal structure of HP0197-G5

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U
Synchrotron site	SSRF
Beamline	BL17U
Temperature [K]	298
Detector technology	IMAGE PLATE
Collection date	2010-05-10
Detector	MAR555 FLAT PANEL
Wavelength(s)	0.9792
Spacegroup name	P 41 2 2
Unit cell lengths	114.592, 114.592, 128.545
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	34.880 - 2.500
R-factor	0.255
Rwork	0.255
R-free	0.27800
RMSD bond length	0.007
RMSD bond angle	1.500
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHENIX
Refinement software	CNS (1.2)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.590
High resolution limit [Å]	2.500	2.490
Number of reflections	29561
Completeness [%]	86.2	91.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION	4.5	293	38% MPD, 0.1M acetate pH 4.5, 0.1M NBSD-256, VAPOR DIFFUSION, temperature 293K