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4FTJ

Crystal Structure of the CHK1

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU RU200
Temperature [K]110
Detector technologyIMAGE PLATE
DetectorMARRESEARCH
Wavelength(s)1.54
Spacegroup nameP 1 21 1
Unit cell lengths45.415, 65.915, 58.236
Unit cell angles90.00, 94.53, 90.00
Refinement procedure
Resolution19.620 - 2.200
R-factor0.1816
Rwork0.180
R-free0.20490
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.009
RMSD bond angle0.960
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Refinement softwareBUSTER-TNT (BUSTER 2.11.1)
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]20.00020.0002.280
High resolution limit [Å]2.2004.7202.200
Rmerge0.0940.0820.226
Number of reflections16827
<I/σ(I)>10.4
Completeness [%]96.992.992.5
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP7.5298PEG 8000, Isopropanol, HEPES, pH 7.5, VAPOR DIFFUSION, SITTING DROP, temperature 298.0K

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