Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 21-ID-F |
| Synchrotron site | APS |
| Beamline | 21-ID-F |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2011-06-16 |
| Detector | MARMOSAIC 225 mm CCD |
| Wavelength(s) | 0.97872 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 57.389, 61.910, 61.341 |
| Unit cell angles | 90.00, 103.24, 90.00 |
Refinement procedure
| Resolution | 29.855 - 2.150 |
| R-factor | 0.2178 |
| Rwork | 0.215 |
| R-free | 0.26220 |
| Structure solution method | SAD |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.763 |
| Data reduction software | HKL-3000 |
| Data scaling software | HKL-3000 |
| Phasing software | PHENIX |
| Refinement software | PHENIX ((phenix.refine: 1.8_1066)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 29.855 | 2.030 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Number of reflections | 28239 | |
| <I/σ(I)> | 15.76 | 3.75 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 7.7 | 7.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7.3 | 298 | 1.4 M SODIUM CITRATE, 0.1 M HEPES PH 7.3, VAPOR DIFFUSION, SITTING DROP, temperature 298K |
