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4FJJ

RB69 DNA polymerase ternary complex with dTTP/dC

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 24-ID-E
Synchrotron siteAPS
Beamline24-ID-E
Temperature [K]110
Detector technologyCCD
Collection date2011-10-15
DetectorAPEX II CCD
Wavelength(s)0.97
Spacegroup nameP 21 21 21
Unit cell lengths75.196, 119.818, 130.637
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution49.310 - 1.990
R-factor0.18576
Rwork0.184
R-free0.22518
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.007
RMSD bond angle1.132
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareAMoRE
Refinement softwareREFMAC (5.5.0109)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.070
High resolution limit [Å]1.9901.990
Number of reflections76430
Completeness [%]94.599.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION6.5298150 mM CaCl2, 10% (w/v) PEG 350 monomethyl ether (MME), and 100 mM sodium cacodylate pH 6.5 , VAPOR DIFFUSION, temperature 298K

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