4F6O

Crystal structure of the yeast metacaspase Yca1

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U
Synchrotron site	SSRF
Beamline	BL17U
Temperature [K]	100
Detector technology	CCD
Collection date	2011-06-25
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.9958
Spacegroup name	H 3
Unit cell lengths	114.627, 114.627, 62.101
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	33.090 - 1.681
R-factor	0.1713
Rwork	0.170
R-free	0.18720
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	3bij
RMSD bond length	0.007
RMSD bond angle	1.144
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	PHENIX ((phenix.refine: 1.7.3_928))

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	1.680
Number of reflections	34430
Completeness [%]	99.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1