4ER4
HIGH-RESOLUTION X-RAY ANALYSES OF RENIN INHIBITOR-ASPARTIC PROTEINASE COMPLEXES
Experimental procedure
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 53.700, 74.000, 45.500 |
| Unit cell angles | 90.00, 109.30, 90.00 |
Refinement procedure
| Resolution | 20.000 - 2.100 |
| R-factor | 0.194 * |
| Rwork | 0.194 |
| RMSD bond length | 0.020 |
| RMSD bond angle | 0.043 |
| Refinement software | PROLSQ |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * | 6.3 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | sodium phosphate | 0.1 (M) | dihydrogen, can be replaced with 0.1M sodium acetate |
| 2 | 1 | 1 | ammonium sulfate | 2.7 (M) | |
| 3 | 1 | 1 | acetone | 10 (%) |
