4EPQ
canonical poly(ADP-ribose) glycohydrolase RBPI inhibitor complex from Tetrahymena thermophila
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04 |
| Synchrotron site | Diamond |
| Beamline | I04 |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 41 |
| Unit cell lengths | 80.680, 80.680, 89.420 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 36.771 - 2.399 |
| R-factor | 0.1683 |
| Rwork | 0.165 |
| R-free | 0.23070 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4epp |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.151 |
| Refinement software | PHENIX ((phenix.refine: 1.7_650)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 36.771 |
| High resolution limit [Å] | 2.399 |
| Number of reflections | 22497 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
