4EKE
Crystal structure of GPb in complex with DK11
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SEALED TUBE |
Source details | OXFORD DIFFRACTION ENHANCE ULTRA |
Temperature [K] | 293 |
Detector technology | CCD |
Collection date | 2011-10-07 |
Detector | AGILENT ATLAS CCD |
Wavelength(s) | 1.5419 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 128.474, 128.474, 116.382 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 13.660 - 2.600 |
R-factor | 0.16168 |
Rwork | 0.158 |
R-free | 0.23088 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 3sym |
RMSD bond length | 0.017 |
RMSD bond angle | 1.715 |
Data reduction software | CrysalisPro |
Data scaling software | SCALA |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 13.900 | 2.740 |
High resolution limit [Å] | 2.600 | 2.600 |
Number of reflections | 30115 | |
<I/σ(I)> | 9.7 | 1.7 |
Completeness [%] | 98.9 | 99.3 |
Redundancy | 3.5 | 2.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | SMALL TUBES | 6.7 | 289 | 10mM BES buffer, pH 6.7, SMALL TUBES, temperature 289K |