4EK7
High speed X-ray analysis of plant enzymes at room temperature
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 295 |
| Detector technology | PIXEL |
| Collection date | 2009-04-29 |
| Detector | PSI PILATUS 6M |
| Wavelength(s) | 1 |
| Spacegroup name | I 2 2 2 |
| Unit cell lengths | 105.560, 129.524, 216.643 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 47.750 - 2.300 |
| R-factor | 0.15332 |
| Rwork | 0.151 |
| R-free | 0.19231 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2jf7 |
| RMSD bond length | 0.021 |
| RMSD bond angle | 2.007 |
| Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 111.170 |
| High resolution limit [Å] | 2.300 |
| Number of reflections | 62803 |
| Completeness [%] | 99.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
