4E1A
Phosphopantetheine adenylyltransferase from Mycobacterium tuberculosis at 1.62A resolution
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL41XU |
Synchrotron site | SPring-8 |
Beamline | BL41XU |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-10-09 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 0.8 |
Spacegroup name | H 3 2 |
Unit cell lengths | 98.734, 98.734, 113.630 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 15.774 - 1.620 |
R-factor | 0.1733 |
Rwork | 0.171 |
R-free | 0.21530 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 0.954 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.000 |
High resolution limit [Å] | 1.580 |
Number of reflections | 29273 |
Completeness [%] | 99.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | COUNTER-DIFFUSION | 273 | COUNTER DIFFUSION, temperature 273K |