4DZZ
Structure of ParF-ADP, crystal form 1
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALS BEAMLINE 8.3.1 |
| Synchrotron site | ALS |
| Beamline | 8.3.1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2011-03-12 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 1.02 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 39.500, 78.300, 68.500 |
| Unit cell angles | 90.00, 93.00, 90.00 |
Refinement procedure
| Resolution | 39.450 - 1.800 |
| R-factor | 0.203 |
| Rwork | 0.203 |
| R-free | 0.24400 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.005 |
| RMSD bond angle | 1.100 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | CNS (1.2) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 78.300 | 1.880 |
| High resolution limit [Å] | 1.800 | 1.800 |
| Number of reflections | 34196 | |
| Completeness [%] | 99.0 | 99 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 298 | peg 4000, isopropanol, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
