4DZK
A de novo designed Coiled Coil CC-Tri-N13
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-02-20 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.98 |
Spacegroup name | P 3 2 1 |
Unit cell lengths | 38.150, 38.150, 44.300 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 44.300 - 1.790 |
R-factor | 0.23174 |
Rwork | 0.230 |
R-free | 0.26899 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.033 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.300 | 1.900 |
High resolution limit [Å] | 1.790 | 1.800 |
Number of reflections | 3777 | |
Completeness [%] | 99.7 | 100 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 2.0 M (NH4)2SO4, 5 % v/v 2-propanol, VAPOR DIFFUSION, SITTING DROP, temperature 291K |