4DYS

Crystal Structure of Apo Swine Flu Influenza Nucleoprotein

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Detector technology	PIXEL
Detector	PSI PILATUS 6M
Spacegroup name	P 61 2 2
Unit cell lengths	94.345, 94.345, 603.804
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	51.850 - 2.800
R-factor	0.2431
Rwork	0.241
R-free	0.29570
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.006
RMSD bond angle	0.820
Data scaling software	XSCALE
Refinement software	REFMAC

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	100.504		2.990
High resolution limit [Å]	2.800	18.940	2.800
Rmerge	0.093	0.017	0.741
Number of reflections	40256	82	4400
<I/σ(I)>	14.22	61.63	2.02
Completeness [%]	94.5	78.8	96.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1