4DWZ
Crystal Structure of Ton_0340
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PAL/PLS BEAMLINE 4A |
| Synchrotron site | PAL/PLS |
| Beamline | 4A |
| Temperature [K] | 110 |
| Detector technology | CCD |
| Collection date | 2010-10-23 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 1.2822 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 107.442, 107.442, 355.031 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 48.920 - 2.700 |
| Rwork | 0.223 |
| R-free | 0.27010 |
| Structure solution method | SAD |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.400 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | SHELXS |
| Refinement software | CNS (1.3) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.750 |
| High resolution limit [Å] | 2.700 | 2.700 |
| Rmerge | 0.364 | |
| Number of reflections | 57476 | |
| <I/σ(I)> | 40.125 | 4.286 |
| Completeness [%] | 98.6 | 98.4 |
| Redundancy | 18 | 11 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 293.15 | 0.1M sodium acetate pH 5.5, 0.35M zinc acetate, 5% isopropanol, VAPOR DIFFUSION, HANGING DROP, temperature 293.15K |
