4DT2

Crystal structure of red kidney bean purple acid phosphatase in complex with Maybridge fragment CC27209

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	AUSTRALIAN SYNCHROTRON BEAMLINE MX2
Synchrotron site	Australian Synchrotron
Beamline	MX2
Detector technology	CCD
Detector	ADSC QUANTUM 315r
Spacegroup name	P 31 2 1
Unit cell lengths	126.760, 126.760, 298.954
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	19.720 - 2.700
R-factor	0.178
Rwork	0.175
R-free	0.22800
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.008
RMSD bond angle	1.144
Refinement software	PHENIX ((phenix.refine: 1.7_650))

Data quality characteristics

	Overall
Low resolution limit [Å]	19.901
High resolution limit [Å]	2.700
Number of reflections	420125

Crystallization Conditions

crystal ID	method	pH	temperature	details
1