4DPN
Crystal Structure of ConM Complexed with Resveratrol
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | LNLS BEAMLINE D03B-MX1 |
| Synchrotron site | LNLS |
| Beamline | D03B-MX1 |
| Temperature [K] | 293 |
| Detector technology | CCD |
| Collection date | 2008-03-16 |
| Detector | MAR CCD 130 mm |
| Wavelength(s) | 1.425 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 119.770, 67.500, 70.460 |
| Unit cell angles | 90.00, 125.86, 90.00 |
Refinement procedure
| Resolution | 27.710 - 2.550 |
| R-factor | 0.1649 |
| Rwork | 0.160 |
| R-free | 0.25465 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.835 |
| Data reduction software | iMOSFLM |
| Data scaling software | SCALA |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 27.710 |
| High resolution limit [Å] | 2.550 |
| Number of reflections | 14216 |
| Completeness [%] | 99.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | Hepes-Na, ammonium sulfate, PEG 400, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
