4DMD
GCN4 leucine zipper domain in a dimeric oligomerization state
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-09-19 |
Detector | RIGAKU SATURN 944 |
Wavelength(s) | 1.5418 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 83.449, 30.478, 27.816 |
Unit cell angles | 90.00, 104.48, 90.00 |
Refinement procedure
Resolution | 40.400 - 2.000 |
R-factor | 0.2366 |
Rwork | 0.235 |
R-free | 0.26485 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2zta |
RMSD bond length | 0.016 |
RMSD bond angle | 1.817 |
Data reduction software | d*TREK |
Data scaling software | d*TREK |
Phasing software | PHASER |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 40.400 |
High resolution limit [Å] | 2.000 |
Rmerge | 0.058 |
Number of reflections | 4757 |
<I/σ(I)> | 15.5 |
Completeness [%] | 99.8 |
Redundancy | 3.76 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 298 | 0.1M Sodium Acetate, 0.1M Sodium Citrate Tribasic Dihydrate, 30% w/v PEG 4000, pH 5.6, VAPOR DIFFUSION, HANGING DROP, temperature 298K |