4CW8
Structure of the carboxy-terminal domain of the turkey type 3 siadenovirus fibre, virulent form
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALBA BEAMLINE XALOC |
| Synchrotron site | ALBA |
| Beamline | XALOC |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2013-07-26 |
| Detector | DECTRIS PILATUS 6M |
| Spacegroup name | I 2 3 |
| Unit cell lengths | 98.963, 98.963, 98.963 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 30.000 - 2.300 |
| R-factor | 0.19903 |
| Rwork | 0.197 |
| R-free | 0.23888 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3zpe |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.553 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Refinement software | REFMAC (5.8.0069) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 31.300 | 2.420 |
| High resolution limit [Å] | 2.300 | 2.300 |
| Rmerge | 0.060 | 0.530 |
| Number of reflections | 7327 | |
| <I/σ(I)> | 6.3 | 1.4 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 8.9 | 9.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7 | 10MM [2-(N-MORPHOLINO)ETHANESULFONIC ACID]-NAOH PH 6.0, 1M (NH4)2HPO4, 0.1 M IMIDAZOLE PH 7.0 |
