4CVS
Structure of Apobacterioferritin Y45F variant
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04 |
| Synchrotron site | Diamond |
| Beamline | I04 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2011-11-05 |
| Detector | ADSC CCD |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 103.490, 27.840, 56.760 |
| Unit cell angles | 90.00, 119.18, 90.00 |
Refinement procedure
| Resolution | 49.557 - 1.392 |
| R-factor | 0.204 |
| Rwork | 0.203 |
| R-free | 0.22490 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2vxi |
| RMSD bond length | 0.019 |
| RMSD bond angle | 1.892 |
| Data reduction software | XDS |
| Data scaling software | TRUNCATE |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 49.560 | 1.400 |
| High resolution limit [Å] | 1.390 | 1.390 |
| Rmerge | 0.070 | 0.310 |
| Number of reflections | 26385 | |
| <I/σ(I)> | 8.32 | 2.02 |
| Completeness [%] | 92.0 | 74.5 |
| Redundancy | 2.63 | 1.79 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
