4CVP
Structure of Apobacterioferritin
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04 |
| Synchrotron site | Diamond |
| Beamline | I04 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2011-11-05 |
| Detector | ADSC CCD |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 95.970, 28.300, 54.470 |
| Unit cell angles | 90.00, 103.48, 90.00 |
Refinement procedure
| Resolution | 46.640 - 2.110 |
| R-factor | 0.21938 |
| Rwork | 0.216 |
| R-free | 0.29877 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2vxi |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.484 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 46.660 | 2.150 |
| High resolution limit [Å] | 2.100 | 2.100 |
| Rmerge | 0.060 | 0.430 |
| Number of reflections | 8475 | |
| <I/σ(I)> | 11.16 | 1.81 |
| Completeness [%] | 99.0 | 99.5 |
| Redundancy | 2.63 | 2.66 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
