4CUR
Crystal structure of human BAZ2B in complex with fragment-3 N09555
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I02 |
| Synchrotron site | Diamond |
| Beamline | I02 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2012-05-17 |
| Detector | DECTRIS PIXEL |
| Spacegroup name | C 2 2 21 |
| Unit cell lengths | 81.100, 96.600, 57.930 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 40.550 - 1.842 |
| R-factor | 0.1727 |
| Rwork | 0.171 |
| R-free | 0.20190 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.003 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.300 | 1.890 |
| High resolution limit [Å] | 1.840 | 1.840 |
| Rmerge | 0.050 | 0.760 |
| Number of reflections | 20037 | |
| <I/σ(I)> | 20.1 | 3.1 |
| Completeness [%] | 99.6 | 99 |
| Redundancy | 8 | 7.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 6.5 | 31% PEG SMEAR LOW, 0.1M MES PH 6.5 |
