4CPV

REFINED CRYSTAL STRUCTURE OF CALCIUM-LIGANDED CARP PARVALBUMIN 4.25 AT 1.5-ANGSTROMS RESOLUTION

Experimental procedure

Spacegroup name	C 1 2 1
Unit cell lengths	28.460, 61.000, 54.400
Unit cell angles	90.00, 95.00, 90.00

Refinement procedure

Resolution	10.000 * - 1.500
R-factor	0.215
RMSD bond length	0.024
RMSD bond angle	1.900
Refinement software	PROLSQ

Data quality characteristics

	Overall
Low resolution limit [Å]	10.000 *
High resolution limit [Å]	1.500 *
Rmerge	0.081 *
Number of reflections	12653 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein solution		0.01-0.04ml
2	1	drop	ammonium sulphate	65-70 (%sat)
3	1	drop	PIPES	10 (mM)
4	1	reservoir	ammonium sulfate