4CP0
Crystal Structure of Epithelial Adhesin 9 A domain (Epa9A) from Candida glabrata in complex with Lactose
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.1 |
Synchrotron site | BESSY |
Beamline | 14.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-11-16 |
Detector | MARRESEARCH MX-255 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 66.580, 66.580, 117.950 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 41.230 - 2.150 |
R-factor | 0.1654 |
Rwork | 0.164 |
R-free | 0.19381 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PRUNED VERSION OF PDB ENTRY 4AF9 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.225 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.230 | 2.270 |
High resolution limit [Å] | 2.150 | 2.150 |
Rmerge | 0.100 | 0.590 |
Number of reflections | 17016 | |
<I/σ(I)> | 24.9 | 4.9 |
Completeness [%] | 99.9 | 100 |
Redundancy | 10.9 | 11.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 0.1 M HEPES PH7, 32% PEG 6000, 0.05 M LACTOSE, VAPOR DIFFUSION IN SITTING DROP |